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功能代谢组学揭示黄芪多糖通过2-羟基丁酸改善肥胖小鼠的脂质代谢 Article

李冰冰, 洪颖, 顾彧, 叶圣洁, 胡凯莉, 姚建, 丁侃, 赵爱华, 贾伟, 李后开

《工程（英文）》 2022年第9卷第2期页码 111-122 doi: 10.1016/j.eng.2020.05.023

摘要：然后，代谢组学分析显示，补充APS 可逆转HFD 诱导的代谢变化，并确定2-羟基丁酸（2-hydroxybutyric acid, 2-HB）是APS活性的潜在功能性代谢产物，该代谢物被HFD显著降低，进一步研究表明，2-HB可抑制油酸（oleic acid, OA）诱导的甘油三酯（triglyceride, TG）累积。还发现其可刺激肝细胞中脂质降解蛋白的表达和3T3-L1 细胞中的TG脂解。此外，在高脂肪和高蔗糖（high-fat and high-sucrose, HFHS）喂养的小鼠中发现2-HB可降低血清TG并调节参与脂质降解的蛋白质。总之，我们的研究表明，APS的代谢
益处至少部分归因于2-HB 的产生，2-HB 在体外和体内均可调节脂质代谢。

关键词：黄芪多糖功能代谢组学 2-羟基丁酸肥胖

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Synthesis of copolymers of 3-acryloyloxymethyl-3′-methyloxetane and 3-(2-(2-(2-Methoxyethylenoxy)ethylenoxy

YE Lin, ZHAO Yumei, FENG Zengguo, BAI Ying, WU Feng

《化学科学与工程前沿（英文）》 2007年第1卷第4期页码 343-348 doi: 10.1007/s11705-007-0062-0

摘要： An oxetane-derived monomer, 3-acryloyloxymethyl-3′-methyloxetane (AMO) was prepared from the reaction of 3-hydromethyl-3-methyloxetane with acryloyl chloride. The cationic ring-opening copolymerization of AMO with another oxetane-derived monomer, 3-(2-(2-(2-methoxyethylenoxy)ethylenoxy)ethylenoxy)-3′-methyloxetane (MEMO) was conducted in CHCl solution using BF3 ·OEt/1, 4-butanediol as a co-initiator. The resulting copolymers were characterized by FTIR, H NMR and Gel Permeation Chromatography (GPC) analyses, and it was found that the enchained ratio of AMO in the copolymers is far lower than its feed ratio. They were crosslinked via the radical polymerization of the vinyl group initiated by BPO after doping with lithium trifluoromethanesulfonimide (LiTFSI) to give rise to tough polymeric electrolyte films. The ionic conductivity was measured at varying content of AMO and different concentration of lithium salt LiTFSI by AC impedance, and a maximum ion conductivity of 1.44×10 S/cm at 30°C or 1.25×10 S/cm at 80°C was attained in the sample PAM 33 at the mole ratio of O : Li = 20. The DSC results indicated that decreases with the increase of the proportion of AMO in the copolymer, well consistent with the ion conductivity trend. The TGA (thermogravimetric analysis) measurement revealed that this kind of copolymer electrolytes is more thermostable than their liquid counterparts.

关键词： 4-butanediol 2-methoxyethylenoxy consistent oxetane-derived copolymer

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Improvement in the synthesis of 2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid 2-benzothiazolyl

GAO Shihao, SUN Chenghui, ZHAO Xinqi, GAO Changquan

《化学科学与工程前沿（英文）》 2008年第2卷第1期页码 80-84 doi: 10.1007/s11705-008-0017-0

摘要： 2-(5-Amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid 2-benzothiazolyl thioester(III), an important intermediate of the fourth generation cephalosporins, was efficiently synthesized by reacting 2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid (I) with 2,2′-dibenzothiazole disulfide (II) in the presence of triphenylphosphine. Effects of reaction time, temperature, solvents, catalysts and feeding molar ratio on the yield and quality of products were investigated, and an improved procedure suitable for industrial production was established. Using 1,2-dichloroethane as solvent, triphenylphosphine as reducer, and triethylamine as catalyst, (I) : (II) : (triphenylphosphine) = 1.0 : 1.0 : 1.0, the product was obtained at room temperature in 98.1% yield. The purity of the product without further purification is 98.7% determined by HPLC method. This procedure could be a suitable alternative to the traditional processes because of its easy handling, high yield and low cost.

关键词： 5-Amino-1 2 4-thiadiazol-3-yl 1 2-dichloroethane important intermediate 2-benzothiazolyl thioester temperature

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Carbonation depth prediction of fly ash concrete subjected to 2- and 3-dimensional CO attack

CHEN Shudong, SUN Wei, ZHANG Yunsheng, GUO Fei

《结构与土木工程前沿（英文）》 2008年第2卷第4期页码 395-400 doi: 10.1007/s11709-008-0046-2

摘要： Based on accelerated carbonation test, 1D, 2D and 3D carbonation of high performance concrete with different fly ash contents (0%, 15%, 20%, 40%, 60%) were studied. The interaction coefficients of 2D and 3D carbonation are defined. The time-dependent coefficient of carbon dioxide diffusion and the interaction coefficients of 2D and 3D carbonation are analyzed. The mathematical model which includes and is deduced. The experiments indicate that 2D and 3D carbonation have obvious interaction. Interaction coefficients obey the attenuation function through time . The mathematical model of 2D and 3D carbonation life prediction based on Fick scattering law can be solved by Fourier expansion. The life prediction of concrete of Sutong Bridge beam shows that the 1D, 2D, 3D carbonation prediction life are 1595 a, 882 a and 758 a, respectively, 2D and 3D carbonation life predicted are reduced clearly.

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Measurement and correlation of the solid-liquid equilibrium of 2-(

Yanhong SUN, Zhiyong LI, Chuang XIE, Wei CHEN, Cui ZHANG

《化学科学与工程前沿（英文）》 2013年第7卷第1期页码 110-115 doi: 10.1007/s11705-013-1316-7

摘要： In this work, the enthalpy of fusion and melting points of 2-( -butyl)-5-methylphenol (2B5MP) and 2-( -butyl)-4-methylphenol (2B4MP) were measured by differential scanning calorimetry (DSC). The binary solid-liquid equilibrium (SLE) of both compounds were predicted by integrated computer aided system (ICAS) and measured by DSC. The corresponding eutectic molar composition is 0.6998 and the eutectic temperature is 281.96 K. The quasi-static heat capacities of 2B5MP and 2B4MP were evaluated by stochastic temperature modulation DSC technique (TOPEM). The SLE experimental data were correlated using the Margules, Wilson, and non-random two liquid (NRTL) equations and a good agreement between measurement and calculation could be obtained.

关键词： solid-liquid equilibrium (SLE) eutectic integrated computer aided system (ICAS) TOPEM correlation

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Synthesis, molecular docking and antibacterial evaluation of 2-(4-(4-aminophenylsulfonyl)phenylamino)-3-(thiophen-2-ylthio)naphthalene-1,4-dione derivatives

Palanisamy RAVICHANDIRAN, Dhanaraj PREMNATH, Samuel VASANTHKUMAR

《化学科学与工程前沿（英文）》 2015年第9卷第1期页码 46-56 doi: 10.1007/s11705-015-1506-6

摘要： A new series of 2-(4-(4-aminophenylsulfonyl)phenylamino)-3-(thiophen-2-ylthio)naphthalene-1,4-dione derivatives ( 3a-3n) were synthesized and characterized by spectral techniques. To understand the interaction of binding sites with bacterial protein receptor, the docking study was performed by the GLIDE program and compound -(4-(4-(1,4-dioxo-3-(thiophen-2-ylthio)-1,4-dihydronaphthalen-2-ylamino)phenylsulfonyl)phenyl)-3-methylbenzamide ( 3b) exhibited good glide and E model scores of ?5.89 and ?94.90, respectively. Moreover among all the molecules studied including the standards used, namely Sparfloxacin (4.8 μg/mL) and Norfloxacin (no inhibition observed) for their antibacterial property, compound -(4-(4-(1,4-dioxo-3-(thiophen-2-ylthio)-1,4-dihydronaphthalen-2-ylamino)phenylsulfonyl)phenyl)-4-nitrobenzamide ( 3e) exhibited the lowest minimum inhibitory concentration (MIC) value of 1.3 μg/mL against .

关键词： MIC 2-thiophene thiol water as solvent acid chlorides sulfone

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类差分平衡函数的性质及其应用

张文英,李世取

《中国工程科学》 2004年第6卷第3期页码 45-52

摘要：

定义了布尔函数的类差分和类差分平衡函数，研究了类差分平衡函数的密码学性质以及构造方法。作为类差分平衡函数的应用，给出了〓上逻辑函数是完全非线性函数的充要条件，并在首先分析得到所有四元类差分平衡函数的基础上，编程搜索出〓上所有的完全非线性函数。

关键词： Bent函数完全非线性函数 2-基展开类差分类自相关函数类差分平衡函数

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趋化信号接枝的掺镁羟基磷灰石促进间充质干细胞归巢

Alessandro Pistone, Daniela Iannazzo, Claudia Espro, Signorino Galvagno, Anna Tampieri, Monica Montesi, Silvia Panseri, Monica Sandri

《工程（英文）》 2017年第3卷第1期页码 55-59 doi: 10.1016/J.ENG.2017.01.007

摘要：本文以人纤连蛋白片段III1-C(FF III1-C) 及纤连蛋白类似物的肽序列Gly-Arg-Gly-Asp-Ser-Pro-Lys 作为趋化因子，分别共价结合至掺镁羟基磷灰石中，用于研究模拟肽序列接枝的掺镁羟基磷灰石对间充质细胞归巢的调控作用用于检测间充质干细胞活力的MTT 法初步研究发现释放趋化信号的掺镁羟基磷灰石可有效促进干细胞迁移。

关键词：掺镁羟基磷灰石间充质干细胞趋化/ 趋触因子骨组织工程

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袁佳欣, 程肖帝, 雷超君, 杨彬, 李中坚, 罗坤, K.H. Koko Lam, 雷乐成, 侯阳, Kostya Ken Ostrikov

《工程（英文）》 2021年第7卷第9期页码 1306-1312 doi: 10.1016/j.eng.2020.01.018

摘要：鉴于此，我们通过将泡沫镍（NF）浸入Fe(NO₃)₃溶液，在泡沫镍基底上原位制备了三维（3D）双金属羟基氧化物杂化物（NiFeOOH/NF）。在这种独特的3D结构中，NiFeOOH/NF 杂化物由均匀生长在NF表面的晶态Ni(OH)₂和无定形FeOOH物种组成。作为双金属羟基氧化物电催化剂，NiFeOOH/NF杂化物表现出优异的电催化OER活性，其性能不仅超过被报道的其他Ni-Fe 基电催化剂，而且超过商业Ir/C 催化剂。1.51 V的应用电势就能分别达到100 mA·cm^{﹣2^{和500 mA·cm^﹣^2<}}

关键词：双金属羟基氧化物析氧反应协同效应高电流密度

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第三届环境、工业和能源工程国际会议(EI2E 2019)

会议日期： 2019年09月19日

会议地点：宁夏银川

主办单位： APISE

第四届设计、机械和材料工程国际会议(D2ME 2019)

会议日期： 2019年09月26日

会议地点：釜山，韩国

主办单位： HKSME

水力空化反应器的最新进展——空化机理、反应器设计与应用 Review

Haoxuan Zheng, Ying Zheng, Jesse Zhu

《工程（英文）》 2022年第19卷第12期页码 180-198 doi: 10.1016/j.eng.2022.04.027

摘要：

水力空化因其能效高、操作成本低、能够诱导化学反应并可规模化等优势，被认为是一种很有前途的工艺强化技术。近十年来，人们对水力空化及其主要变量的基本认识取得了一些进展，为水力空化在自由基诱导化学反应过程中的应用提供了基础。在这里，我们对这些研究工作进行了广泛回顾，包括水力空化的基本原理、空化反应器的设计、空化诱导的反应增强及相关的工业应用。比较了两种类型的水力空化反应器，即固定式和旋转式水力空化反应器。讨论了水力空化反应器的设计参数及其在实验室和中试尺度上的反应器性能，并就其最佳操作和几何条件提出了建议。本文首次回顾了目前市场上的商业空化反应器。水力空化的独特特点已广泛应用于各种化学反应，如氧化反应和废水处理，以及如乳化液生成和组分提取等物理过程。文中也详细讨论了自由基和气泡内爆的作用。

关键词：水动力空化作用空化核羟基自由基固定/旋转水动力空化反应器反应增强空化应用

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单萜类化合物芳樟醇、甲基丁香酚、草蒿脑和香茅醛对配体门控离子通道的作用模式 Article

Amy S. Li, Akimasa Iijima, Junhao Huang, Qing X. Li, Yongli Chen

《工程（英文）》 2020年第6卷第5期页码 541-545 doi: 10.1016/j.eng.2019.07.027

摘要：众所周知，γ-氨基丁酸A型受体（GABAAR）和烟碱型乙酰胆碱受体（nAChR）是目前市场上使用的合成杀虫剂的主要分子靶标。LL是GABAAR的一种浓度依赖性、非竞争性抑制剂，因为在实验中我们发现，小鼠α1β3γ2L GABAAR的γ-氨基丁酸（GABA）半最大效应浓度（EC50

关键词：精油 γ-氨基丁酸A型受体芳樟醇单萜烟碱型乙酰胆碱受体

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肖永红：临床高耐药与高毒性病原体共进化（2023年2月22日）

2023年03月10日

关键词：代谢与免疫

第四届设计、机械和材料工程国际会议(D2ME 2019)

会议日期： 2019年09月26日

会议地点：釜山，韩国

主办单位： HKSME

标题作者时间类型操作

功能代谢组学揭示黄芪多糖通过2-羟基丁酸改善肥胖小鼠的脂质代谢

李冰冰, 洪颖, 顾彧, 叶圣洁, 胡凯莉, 姚建, 丁侃, 赵爱华, 贾伟, 李后开

期刊论文

Synthesis of copolymers of 3-acryloyloxymethyl-3′-methyloxetane and 3-(2-(2-(2-Methoxyethylenoxy)ethylenoxy

YE Lin, ZHAO Yumei, FENG Zengguo, BAI Ying, WU Feng

期刊论文

Improvement in the synthesis of 2-(5-amino-1,2,4-thiadiazol-3-yl)-2-(Z)-methoxyiminoacetic acid 2-benzothiazolyl

GAO Shihao, SUN Chenghui, ZHAO Xinqi, GAO Changquan

期刊论文

Carbonation depth prediction of fly ash concrete subjected to 2- and 3-dimensional CO attack

CHEN Shudong, SUN Wei, ZHANG Yunsheng, GUO Fei

期刊论文

Measurement and correlation of the solid-liquid equilibrium of 2-(

Yanhong SUN, Zhiyong LI, Chuang XIE, Wei CHEN, Cui ZHANG

期刊论文

Synthesis, molecular docking and antibacterial evaluation of 2-(4-(4-aminophenylsulfonyl)phenylamino)-3-(thiophen-2-ylthio)naphthalene-1,4-dione derivatives

Palanisamy RAVICHANDIRAN, Dhanaraj PREMNATH, Samuel VASANTHKUMAR

期刊论文

类差分平衡函数的性质及其应用

张文英,李世取

期刊论文

趋化信号接枝的掺镁羟基磷灰石促进间充质干细胞归巢

Alessandro Pistone, Daniela Iannazzo, Claudia Espro, Signorino Galvagno, Anna Tampieri, Monica Montesi, Silvia Panseri, Monica Sandri

期刊论文

双金属羟基氧化物——一种应用于工业相关条件下的高性能水氧化电催化剂

袁佳欣, 程肖帝, 雷超君, 杨彬, 李中坚, 罗坤, K.H. Koko Lam, 雷乐成, 侯阳, Kostya Ken Ostrikov

期刊论文

第三届环境、工业和能源工程国际会议(EI2E 2019)